Mass Spectrometry of Polymers by Giorgio Montaudo (2002)

Description

Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results achieved. Mass Spectrometry of Polymers effectively fills this need. The discussion begins by introducing MS in detail, providing a historical perspective and a review of modern instrumentation and methods. The text then focuses on mathematical concepts and practical algorithms used in some of the major quantitative polymer applications of MS, providing a skillful prologue to polymer characterization techniques. Detailed chapters follow, describing the most relevant applications of MS to the analysis of polymers and the techniques currently employed. Authored by internationally recognized experts from academia and industry, Mass Spectrometry of Polymers is the only state-of-the-art work available that deals systematically with this rapidly emerging discipline, and will be useful to both novices and experienced practitioners in polymer MS.

Contents
Preface
Giorgio Montaudo and Robert P. Lattimer
1 Introduction to Mass Spectrometry of Polymers
Michael J. Polce and Chrys Wesdemiotis
2 Polymer Characterization Methods
Giorgio Montaudo and Maurizio S. Montaudo
3 Pyrolysis Gas Chromatography/
Mass Spectrometry (Py-GC/MS)
Shin Tsuge and Hajime Ohtani
4 Electrospray Ionization (ESI-MS) and On-Line Liquid
Chromatography/Mass Spectrometry (LC/MS)
Laszlo Prokai
5 Direct Pyrolysis of Polymers into the Ion Source
of a Mass Spectrometer (DP-MS)
Giorgio Montaudo and Concetto Puglisi
6 Field Ionization (FI-MS) and Field Desorption (FD-MS)
Robert P. Lattimer
7 Fast Atom Bombardment of Polymers (FAB-MS)
Giorgio Montaudo and Filippo Samperi
8 Time-of-Flight Secondary Ion Mass Spectrometry
(TOF-SIMS)
David M. Hercules
9 Laser Fourier Transform Mass Spectrometry (FT-MS)
Salvador J. Pastor and Charles L. Wilkins
10 Matrix-Assisted Laser Desorption/Ionization Mass
Spectrometry of Polymers (MALDI-MS)
Giorgio Montaudo, Maurizio S. Montaudo, and Filippo Samperi
11 Two-Step Laser Desorption Mass Spectrometry
Mattanjah S. de Vries and Heinrich E. Hunziker

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